WORKS & HONORS

Achievements

RESEARCH OUTPUT

Publications

2026

  1. A C3-Symmetric Phloroglucinol Derivative for Tuning the Structures and Luminescence of Solvates
    Iwasaki, A.; Moriyama, Y.; Ito, S.*
    Cryst. Growth Des. 2026, 26, 7584–7594.
    DOI: 10.1021/acs.cgd.6c00616
    TOC graphic for A C 3 -Symmetric Phloroglucinol Derivative for Tuning the Structures and Luminescence of SolvatesTOC image unavailable
  2. Mechanochromic luminescence of organic crystals: current progress and emerging functions
    Ito, S.*
    Bull. Chem. Soc. Jpn. 2026, 99, uoag119.
    DOI: 10.1093/bulcsj/uoag119 (Open Access, Invited Review)
    TOC graphic for Mechanochromic luminescence of organic crystals: current progress and emerging functionsTOC image unavailable
  3. A Proline-Integrated Donor–Acceptor Fluorophore: Water-Vapor-Responsive Mechanochromic Luminescence and Latent Fingerprint Visualization
    Chen, H.; Kato, K.; Imai, Y.*; Ito, S.*
    Adv. Opt. Mater. 2026, 14, e71360.
    DOI: 10.1002/adom.71360 (Open Access)
    TOC graphic for A Proline-Integrated Donor–Acceptor Fluorophore: Water-Vapor-Responsive Mechanochromic Luminescence and Latent Fingerprint VisualizationTOC image unavailable
  4. Doping-activated thermal polymorphic transition of luminescent organic crystals
    Furukawa, H.; Tachikawa, T.; Ito, S.*
    Chem. Commun. 2026, 62, 8008–8012.
    DOI: 10.1039/D6CC00603E
    TOC graphic for Doping-activated thermal polymorphic transition of luminescent organic crystalsTOC image unavailable
  5. A quasiracemic strategy for controlling the guest-inclusion capability of metal–organic structures
    Zhao, Y.; Ito, S.*
    Bull. Chem. Soc. Jpn. 2026, 99, uoag025.
    DOI: 10.1093/bulcsj/uoag025
    TOC graphic for A quasiracemic strategy for controlling the guest-inclusion capability of metal–organic structuresTOC image unavailable
  6. Quantitative evaluation of mechanochromic luminescent materials under controlled grinding stimuli
    Ito, S.*; Nagai, S.; Ikeya, M.; Mashimo, T.; Seki, T.; Ito, H.; Sagara, Y.; Mutai, T.; Ooyama, Y.; Nakano, K.*
    J. Mater. Chem. C 2026, 14, 1384–1394.
    DOI: 10.1039/D5TC03324A
    Selected as Hot Paper, Selected as Front Cover
    ChemRxiv 2025, DOI: 10.26434/chemrxiv-2025-td3c0. (Link)
    TOC graphic for Quantitative evaluation of mechanochromic luminescent materials under controlled grinding stimuliTOC image unavailable

2025

  1. A disilane-bonded bis(methylpyridine) Cu(I) complex exhibiting reversible trigonal–tetrahedral switch with stimuli-responsive luminescence
    Yamanoi, Y.*; Zhao, Y.; Nakae, T.; Segawa, K.; Yoshida, M.; Kato, M.; Kikuchi, K.; Imoto, H.; Naka, K.; Kitajima, S.; Oka, K.; Kasai, H.; Ito, S.*
    Dalton Trans. 2025, 54, 17425–17429.
    DOI: 10.1039/D5DT01893E
  2. Lamellar-Cleavage-Induced Triboluminescence in Discrete Chiral Complexes with Lanthanides
    Ohno, R.; Saso, A.; Yamamoto, Y.; Hayauchi, D.; Ohmagari, H.; Saito, D.; Hattori, S.; Nishimoto, C.; Nakayama, N.; Nakano, K.; Ito, S.; Kawaguchi, S.; Kato, M.; Ishii, K.; Hasegawa, M.*
    Chem. Eur. J. 2025, 31, e02824.
    DOI: 10.1002/chem.202502824
  3. Reprecipitation-driven access to solvates and solvent-free crystals: achieving two-solvent-mediated vapochromic luminescence
    Ogawa, K.; Sumida, A.; Kubota, R.; Tachikawa, T.; Ito, S.*
    CrystEngComm 2025, 27, 7484–7490.
    DOI: 10.1039/D5CE00946D
    Selected as Front Cover
    TOC graphic for Reprecipitation-driven access to solvates and solvent-free crystals: achieving two-solvent-mediated vapochromic luminescenceTOC image unavailable
  4. Tunable Mechanochromic Luminescence of Organic Crystals
    Ito, S.
    Advances in Organic Crystal Chemistry ed. by Kobatake, S.; Uekusa, H.
    DOI: 10.1007/978-981-96-4479-7_6
  5. Quasiracemic Crystallization of Luminescent Chiral Molecules: Mechanochromic Luminescence and Sign Inversion of Circularly Polarized Luminescence
    Ito, S.*; Fukuhara, K.; Arakawa, N.; Suzuki, S.; Imai, Y.*
    Chem. Eur. J. 2025, 31, e202501677.
    DOI: 10.1002/chem.202501677 (Open Access)
    Selected as Front Cover
    TOC graphic for Quasiracemic Crystallization of Luminescent Chiral Molecules: Mechanochromic Luminescence and Sign Inversion of Circularly Polarized LuminescenceTOC image unavailable
  6. Enantiopure and quasiracemic crystals of 7-substituted tryptophan derivatives: modulation of molecular arrangement for functionalized crystals
    Tsuchiya, Y.; Ohata, M.; Chisuga, T.; Nakano, S.; Ito, S.*
    CrystEngComm 2025, 27, 3095–3101.
    DOI: 10.1039/D5CE00099H
    TOC graphic for Enantiopure and quasiracemic crystals of 7-substituted tryptophan derivatives: modulation of molecular arrangement for functionalized crystalsTOC image unavailable
  7. Multi-color luminescent crystals derived from dynamic diastereomers of a perylene-substituted binaphthol derivative
    Yano, R.; Ito, S.*
    Chem. Commun. 2025, 61, 5305–5308.
    DOI: 10.1039/D5CC00758E
    TOC graphic for Multi-color luminescent crystals derived from dynamic diastereomers of a perylene-substituted binaphthol derivativeTOC image unavailable
  8. Contrasting Mechanochromic Luminescence of Enantiopure and Racemic Pyrenylprolinamides: Elucidating Solid-State Excimer Orientation by Circularly Polarized Luminescence
    Ito, S.*; Wakiyama, S.; Chen, H.; Abekura, M.; Uekusa, H.; Ikemura, R.; Imai, Y.*
    Angew. Chem. Int. Ed. 2025, 64, e202422913.
    DOI: 10.1002/anie.202422913 (Open Access)
    Selected as Frontispiece
    Press Release: EurekAlert!, YNU, Kindai Univ., Science Tokyo, JST
    TOC graphic for Contrasting Mechanochromic Luminescence of Enantiopure and Racemic Pyrenylprolinamides: Elucidating Solid-State Excimer Orientation by Circularly Polarized LuminescenceTOC image unavailable
  9. Development of Innovative Luminescent Functional Molecules Based on Fine Organic Synthesis
    Ito, S.*
    J. Synth. Org. Chem. Jpn. 2025, 83, 25–33.
    DOI: 10.5059/yukigoseikyokaishi.83.25
    TOC graphic for Development of Innovative Luminescent Functional Molecules Based on Fine Organic SynthesisTOC image unavailable

2024

  1. Structural and Photophysical Differences in Crystalline Trigonal Planar Copper Iodide Complexes with 1,2-Bis(methylpyridin-2-yl)disilane Ligands
    Zhao, Y.; Nakae, T.; Segawa, K.; Yoshida, M.; Kato, M.; Omoto, K.; Ito, S.*; Yamada, T.*; Yamanoi, Y.*
    Inorg. Chem. 2024, 63, 22361–22371.
    DOI: 10.1021/acs.inorgchem.4c02758
  2. Social Self-Sorting of Quasi-Racemates: A Unique Approach for Dual-Pore Molecular Crystals
    Kimoto, M.; Sugiyama, S.; Kumano, K.; Inagaki, S.; Ito, S.*
    J. Am. Chem. Soc. 2024, 146, 17559–17565.
    DOI: 10.1021/jacs.4c01654 (Open Access)
    Press Release: EurekAlert!, YNU, JST
    TOC graphic for Social Self-Sorting of Quasi-Racemates: A Unique Approach for Dual-Pore Molecular CrystalsTOC image unavailable
  3. Dual-Stimuli-Responsive Turn-On Luminescence of Chiral Bisimidazolyl BINOL Dimethyl Ether Crystals
    Murata, H.; Suzuki, S.; Terakubo, K.; Imai, Y.*; Ito, S.*
    Chem. Asian J. 2024, 19, e202400293.
    DOI: 10.1002/asia.202400293 (Open Access)
    Selected as Front Cover
    Top viewed article
    TOC graphic for Dual-Stimuli-Responsive Turn-On Luminescence of Chiral Bisimidazolyl BINOL Dimethyl Ether CrystalsTOC image unavailable
  4. Fused heteroaromatic donor–acceptor fluorophores: enhanced brightness and variable emission characteristics
    Sumida, A.; Takahashi, S.; Nagai, S.; Ito, S.*
    Chem. Lett. 2024, 53, upae047.
    DOI: 10.1093/chemle/upae047
    TOC graphic for Fused heteroaromatic donor–acceptor fluorophores: enhanced brightness and variable emission characteristicsTOC image unavailable
  5. Self-Recovering Mechanochromic Luminescence
    Ito, S.
    Organic and Inorganic Materials Based Sensors ed. by Das, S.; Thomas, S.; Das, P. P. Wiley-VCH, 2024, Chap. 35, pp. 815–840.
    DOI: 10.1002/9783527834266.ch35

2022

  1. A Series of D‒A‒D Structured Disilane-Bridged Triads: Structure and Stimuli-Responsive Luminescence Studies
    Miyabe, H.; Ujita, M.; Nishio, M.; Nakae, T.; Usuki, T.; Ikeya, M.; Nishimoto, C.; Ito, S.; Hattori, M.; Takeya, S.; Hayashi, S.; Saito, D.; Kato, M.; Nishihara, H.; Yamada, T.; Yamanoi, Y.*
    J. Org. Chem. 2022, 87, 8928–8938.
    DOI: 10.1021/acs.joc.2c00641
  2. Tunable mechanochromic luminescence via surface protonation of pyridyl-substituted imidazole crystals
    Kubota, R.; Yuan, Y.; Yoshida, R.; Tachikawa, T.*; Ito, S.*
    Mater. Adv. 2022, 3, 5826–5835.
    DOI: 10.1039/D2MA00256F (Open Access)
    TOC graphic for Tunable mechanochromic luminescence via surface protonation of pyridyl-substituted imidazole crystalsTOC image unavailable
  3. Extension of the mechanoresponsive luminescence shift via formation of a doped organic crystal
    Yoshida, R.; Tachikawa, T.*; Ito, S.*
    Chem. Commun. 2022, 58, 6781–6784.
    DOI: 10.1039/D2CC00741J
    Selected as Front Cover
    TOC graphic for Extension of the mechanoresponsive luminescence shift via formation of a doped organic crystalTOC image unavailable
  4. Dual-channel recognition of Al3+ and Cu2+ ions using a chiral pyrene-based fluorescent sensor
    Matsuura, Y.; Asami, M.; Ito, S.*
    New J. Chem. 2022, 46, 7864–7871.
    DOI: 10.1039/D2NJ00801G
    Selected as Front Cover
    TOC graphic for Dual-channel recognition of Al 3+ and Cu 2+ ions using a chiral pyrene-based fluorescent sensorTOC image unavailable
  5. Luminescent polymorphic crystals: mechanoresponsive and multicolor-emissive properties
    Ito, S.*
    CrystEngComm 2022, 24, 1112–1126.
    DOI: 10.1039/D1CE01614H (Invited Review)
    Selected as Front Cover, Selected as HOT article
    TOC graphic for Luminescent polymorphic crystals: mechanoresponsive and multicolor-emissive propertiesTOC image unavailable
  6. Mechanochromic luminescence of soft crystals: Recent systematic studies in controlling the molecular packing and mechanoresponsive properties
    Ito, S.*
    J. Photochem. Photobiol., C 2022, 51, 100481.
    DOI: 10.1016/j.jphotochemrev.2021.100481 (Invited Review)
    Special Issue on Soft Crystals
    TOC graphic for Mechanochromic luminescence of soft crystals: Recent systematic studies in controlling the molecular packing and mechanoresponsive propertiesTOC image unavailable
  7. Mechano- and Thermo-responsive Luminescence of Crystalline Thienylbenzothiadiazole Derivatives: Stepwise Hypsochromic Switching of Near-Infrared Emission
    Yoshida, R.; Tachikawa, T.*; Ito, S.*
    Cryst. Growth Des. 2022, 22, 547–558.
    DOI: 10.1021/acs.cgd.1c01128
    Special Issue on Emerging Investigators 2022
    TOC graphic for Mechano- and Thermo-responsive Luminescence of Crystalline Thienylbenzothiadiazole Derivatives: Stepwise Hypsochromic Switching of Near-Infrared EmissionTOC image unavailable

2021

  1. Luminescent Behavior Elucidation of a Disilane-Bridged D‒A‒D Triad Composed of Phenothiazine and Thienopyrazine
    Nakae, T.; Nishio, M.; Usuki, T.; Ikeya, M.; Nishimoto, C.; Ito, S.; Nishihara, H.; Hattori, M.; Hayashi, S.; Yamada, T.; Yamanoi, Y.*
    Angew. Chem. Int. Ed. 2021, 60, 22871–22878.
    DOI: 10.1002/anie.202108089
  2. Mechanochromic Luminescence (MCL) of Purely Organic Two-Component Dyes: Wide-Range MCL over 300 nm and Two-Step MCL by Charge-Transfer Complexation
    Ito, S.*; Sekine, R.; Munakata, M.; Yamashita, M.; Tachikawa, T.*
    Chem. Eur. J. 2021, 27, 13982–13990.
    DOI: 10.1002/chem.202102700 (Read Only Link)
    Selected as Cover Feature
    TOC graphic for Mechanochromic Luminescence (MCL) of Purely Organic Two-Component Dyes: Wide-Range MCL over 300 nm and Two-Step MCL by Charge-Transfer ComplexationTOC image unavailable
  3. In Situ Exploration of Stimulus-Induced Emission Changes in Mechanochromic Dyes
    Yamashita, M.; Nagai, S.; Ito, S.*; Tachikawa, T.*
    J. Phys. Chem. Lett. 2021, 12, 7826–7831.
    DOI: 10.1021/acs.jpclett.1c02015
  4. Multi-color mechanochromic luminescence of three polymorphic crystals of a donor–acceptor-type benzothiadiazole derivative
    Ito, S.*, Nagai, S.; Ubukata, T.; Tachikawa, T.
    CrystEngComm 2021, 23, 5899–5907.
    DOI: 10.1039/D1CE00445J (Open Access)
    Special Issue on Mechanically responsive crystalline materials
    TOC graphic for Multi-color mechanochromic luminescence of three polymorphic crystals of a donor–acceptor-type benzothiadiazole derivativeTOC image unavailable
  5. Mechanochromic Luminescence and Solid-State Circularly Polarized Luminescence of a Chiral Diamine-Linked Bispyrene
    Ito, S.*; Sekine, R.; Munakata, M.; Asami, M.; Tachikawa, T.; Kaji, D.; Mishima, K.; Imai, Y.*
    ChemPhotoChem 2021, 5, 920–925.
    DOI: 10.1002/cptc.202100087 (Read Only Link)
    Selected as Front Cover, Highlighted in Cover Profile
    TOC graphic for Mechanochromic Luminescence and Solid-State Circularly Polarized Luminescence of a Chiral Diamine-Linked BispyreneTOC image unavailable
  6. Recent Advances in Mechanochromic Luminescence of Organic Crystalline Compounds
    Ito, S.*
    Chem. Lett. 2021, 50, 649–660.
    DOI: 10.1246/cl.200874 (Open Access, Invited Review)
    TOC graphic for Recent Advances in Mechanochromic Luminescence of Organic Crystalline CompoundsTOC image unavailable

2015 and Earlier

  1. Enantioselective addition of diethylzinc to aldehydes catalyzed by (R)-1-phenylethylamine-derived 1,4-amino alcohols
    Asami, M.*; Miyairi, N.; Sasahara, Y.; Ichikawa, K.; Hosoda, N.; Ito, S.
    Tetrahedron 2015, 71, 6796–6802.
    DOI: 10.1016/j.tet.2015.07.031
  2. Optical Resolution of C2-Symmetric Racemic 1,4-Diols with o-Xylylene Structure by Chiral Resolving Agent (S)-ALBO-V
    Asami, M.*; Zhong, L.; Sekiguchi, N.; Yamada, K.; Hiwatashi, Y.; Taniguchi, T.; Hosoda, N.; Ito, S.
    Bull. Chem. Soc. Jpn. 2015, 88, 966–968.
    DOI: 10.1246/bcsj.20150066
  3. Enantioselective Addition of Diethylzinc to Aldehydes Catalyzed by Diastereomeric 1,4-Amino Alcohols with o-Xylylene Skeleton
    Asami, M.*; Nagai, A.; Sasahara, Y.; Ichikawa, K.; Ito, S.; Hosoda, N.
    Chem. Lett. 2015, 44, 345–347.
    DOI: 10.1246/cl.141113
  4. Mesoporous aluminosilicate-catalyzed Mukaiyama aldol reaction of aldehydes and acetals
    Ito, S.; Tanuma, K.; Matsuda, K.; Hayashi, A.; Komai, H.; Kubota, Y.; Asami, M.*
    Tetrahedron 2014, 70, 8498–8504.
    DOI: 10.1016/j.tet.2014.09.073
  5. Procedure-Dependent Construction of Two Isomers of Trimeric Self-Assembled Boronic Esters
    Ono, K.; Aizawa, R.; Yamano, T.; Ito, S.; Yasuda, N.; Johmoto, K.; Uekusa, H.; Iwasawa, N.*
    Chem. Commun. 2014, 50, 13683–13686.
    DOI: 10.1039/C4CC05836D
  6. 1,3-Addition of silyl enol ethers to nitrones catalyzed by mesoporous aluminosilicate
    Ito, S.; Kubota, Y.; Asami, M.*
    Tetrahedron Lett. 2014, 55, 4930–4932.
    DOI: 10.1016/j.tetlet.2014.07.020
    Highlighted in Synfacts 2014, 10, 1217
  7. Release and Recovery of Guest Molecules during the Reversible Borate Gel Formation of Guest-Included Macrocyclic Boronic Esters
    Ito, S.; Takata, H.; Ono, K.; Iwasawa, N.*
    Angew. Chem. Int. Ed. 2013, 52, 11045–11048.
    DOI: 10.1002/anie.201303870
  8. Controlled Self-Assembly of Multiple Diastereomeric Macrocyclic Boronic Esters Composed of Two Chiral Units
    Ito, S.; Ono, K.; Iwasawa, N.*
    J. Am. Chem. Soc. 2012, 134, 13962–13965.
    DOI: 10.1021/ja306249f
  9. Mesoporous aluminosilicate-catalyzed allylation of carbonyl compounds and acetals
    Ito, S.; Hayashi, A.; Komai, H.; Yamaguchi, H.; Kubota, Y.; Asami, M.*
    Tetrahedron 2011, 67, 2081–2089.
    DOI: 10.1016/j.tet.2011.01.055
  10. Mesoporous aluminosilicate-catalyzed Sakurai allylation and Mukaiyama aldol reaction of acetals
    Ito, S.; Hayashi, A.; Komai, H.; Kubota, Y.; Asami, M.*
    Tetrahedron Lett. 2010, 51, 4243–4245.
    DOI: 10.1016/j.tetlet.2010.06.034
    Highlighted in Synfacts 2010, 1202
  11. Mukaiyama Aldol Reaction Catalyzed by Mesoporous Aluminosilicate
    Ito, S.; Yamaguchi, H.; Kubota, Y.; Asami, M.*
    Chem. Lett. 2009, 38, 700–701.
    DOI: 10.1246/cl.2009.700
    Highlighted in Synfacts 2009, 1172
  12. Mesoporous aluminosilicate-catalyzed allylation of aldehydes with allylsilanes
    Ito, S.; Yamaguchi, H.; Kubota, Y.; Asami, M.*
    Tetrahedron Lett. 2009, 50, 2967–2969.
    DOI: 10.1016/j.tetlet.2009.04.002
  13. Asymmetric total synthesis of (+)-curcutetraol and (+)-sydonol
    Ito, S.; Zhang, C.; Hosoda, N.; Asami, M.*
    Tetrahedron 2008, 64, 9879–9884.
    DOI: 10.1016/j.tet.2008.08.012
  14. First asymmetric total synthesis of (+)-curcutetraol
    Zhang, C.; Ito, S.; Hosoda, N.; Asami, M.*
    Tetrahedron Lett. 2008, 49, 2552–2554.
    DOI: 10.1016/j.tetlet.2008.02.094

RECOGNITION

Student Awards

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2025.11.27

第15回CSJ化学フェスタ2025 優秀ポスター発表賞

佐藤 真哉

酸蒸気曝露後に誘起される発光性有機結晶の解離的変形

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2025.11.22

第4回ソフトクリスタル研究会 学生発表賞

佐藤 真哉

ピリジル置換発光性ビナフトールソフトクリスタルの酸蒸気や熱による解離的変形

YNU News
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2025.09.06

2025年光化学討論会 最優秀学生発表賞（ポスター）

陳 豪

Water-Vapor-Responsive Mechanochromic Luminescent Proline Derivative

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2025.06.08

第22回ホスト-ゲスト・超分子化学シンポジウム ポスター賞（Chemical Communications賞）

小川 滉太

ゲスト分子の包接と放出を伴うホスト結晶の構造変化とベイポクロミック発光

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2024.11.29

第14回CSJ化学フェスタ2024 優秀ポスター発表賞

矢野 理子

軸回転するペリレン置換ビナフトール誘導体の結晶構造と発光特性

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2024.10.27

第32回有機結晶シンポジウム 最優秀ポスター賞・CrystEngComm Poster Prize

矢野 理子

ペリレン置換ビナフトール誘導体によるジアステレオマー結晶の形成と発光特性

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2024.06.02

第21回ホスト-ゲスト・超分子化学シンポジウム 優秀ポスター賞

矢野 理子

軸回転可能なペリレン置換ビナフトール誘導体による溶媒包接結晶の形成と発光特性

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2023.11.30

第13回CSJ化学フェスタ2023 優秀ポスター発表賞

森山 裕歩

非共役型ドナー・アクセプター色素からなる結晶性薄膜のメカノクロミック発光

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2023.11.24

第2回ソフトクリスタル研究会 学生ポスター発表賞

森山 裕歩

メカノクロミック発光性有機ソフトクリスタルからなる自立薄膜の創製

YNU News
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2023.09.07

2023年光化学討論会 優秀学生発表賞（ポスター）

森山 裕歩

Mechanochromic Luminescent Thin Films Composed of Non-conjugated Donor–acceptor-type Dyes

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2022.11.30

第12回CSJ化学フェスタ2022 優秀ポスター発表賞

杉山 翔一

動的イミン結合を利用したキラルピレノファンの自己組織化と発光特性

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2022.11.20

第1回ソフトクリスタル研究会 優秀ポスター賞

脇山 晋

ピレン環を有するキラルなプロリンアミド結晶のメカノクロミック発光と円偏光発光スイッチング

YNU News
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2021.12.01

第11回CSJ化学フェスタ2021 優秀ポスター発表賞

吉田 遼平

チエニルベンゾチアジアゾール誘導体の段階的刺激応答発光

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2021.09.30

2021年光化学討論会 優秀学生発表賞（ポスター）

吉田 遼平

Tuning the Mechanochromically Luminescent Properties of Thienylbenzothiadiazole by Forming Mixed Crystals

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2019.11.26

スマートマテリアル研究会講演会 若手奨励賞

高橋 昌平

ドナー・アクセプター型複素環式固体発光色素による多彩なメカノクロミック発光

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2019.11.20

第9回CSJ化学フェスタ2019 優秀ポスター発表賞

鈴木 颯人

4-アリールエチニルベンズアルデヒド誘導体による貴金属を用いない水素ガスの蛍光検出

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2016.12.08

第6回CSJ化学フェスタ2016 優秀ポスター発表賞

生田 健悟

多環芳香環を有するキラルな C2 対称ジアミン誘導体によるキラルセンシング

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2015.11.12

第5回CSJ化学フェスタ2015 優秀ポスター発表賞

生田 健悟

キラルな C2 対称ジアミン誘導体の合成とその不斉認識能

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2015.05.16

第69回有機合成化学協会関東支部シンポジウム 若手講演賞

生田 健悟

キラルな C2 対称ジアミン誘導体の合成とそのキラルシフト試薬としての利用